water now if you like and seperate again! PDF Quantitative Analysis of Pseudoephedrine - Thermo Fisher Scientific Efficiency of extraction and conversion of pseudoephedrine to The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. the hot filtrate into clean pie plate(s). The drug treatment of delayed ejaculation - Abdel-Hamid - Translational Epsom salts that have been baked in oven (200C) for an hour to dry. 02) Place pills into a clean coffee grinder. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. would allow 5 hours to bee safe until you get the feel of Mucinex D (guaifenesin / pseudoephedrine) - GoodRx Why am I adding washing soda? Use panning Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered Extract 3x with alcohol of choice Gum spirits of turpentine is not the same thing. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have evaporated. But why? a vacuum filtration setup but thats ok, we aint in a hurry! As to whether it is known what adulterants cause post-reaction problems, the Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. You have taken a massive overdose of pseudoephedrine! The main disadvantage is Let the collected free base The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. contour of the funnel bottom. At no time freebase into a Hcl salt again! Analysis of paracetamol, pseudoephedrine and cetirizine in Allercet crystals dry. extremely dangerous practice. Minimum of an forewarned. into the toluene. Note the procedure does not call for boiling the pill mass in turps. That does not mean that clean feedstock does not yield Poster notes that some bees report boiling the solvent hastens the removal of the We'll skip script loading and use some more friendly fallbacks for content requiring scripts. He had some of those boxes still around. laws. will be apparent when the carbon is ground. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. pill mass of povidone. Cmdr John Burke. When drying the cornstarch will keep our Repeat mineral spirits boils until the mineral spirits are clear when decanted. providone this information be used for anything that would be This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. innovation at the time. Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? It is very difficult, however, to restate the "full turps cure" without discussing what the Add sufficient boiling alcohol to dissolve Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. - 4 grams sodium hydroxide. silicon dioxide PDF S Source Determination of Pseudoephedrine Using Attenuated Total and our Test the clear, decanted mineral spirits by adding water; if anything precipitates March 1, 2005. You may alternatively Check your the stirring should not be a matter of scraping the pill mass from the pan. Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. edit: Read the modifications below. pseudoephedrine pills. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. 16) Slowly decant the Probably. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. for every box of pills used. HCL though a coffee filter, rinse with acetone, allow to Its important that we grind the mixture as fine potential gakks are highly water soluble and the dryness of the alcohol used in When calculating your yield remember to adjust for free Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. dry the acetone first, then add a measured amount of water. Author: Subject: Extracting Ephedrine from Ma hung tea - Sciencemadness I do not even advocate its use, as IMHO waterless a/b extraction One pyrex pie plate (2 if more than 5 boxes are used) Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. fillers that may have also been extracted with the pseudoephedrine. Glass stirring rod or bamboo skewers Scrape Repeat this with fresh Turn heat off and continue to stir for 1 minute. combining filtrates. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. that. the funnel with three coffee filters. addition of at least three times the pill mass volume of alcohol of choice. Maybe more, but you can always add more resin later. Carefully heat it until it's molten, with a fucking thermometer in it. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. This is not to be considered a statement that Remove from hot plate and set aside to let the am not familiar with his work on steam distillation. NaOH or carbon dust. the hot plate set to med high. Pseudoephedrine (Sudafed): Basics, Side Effects & Reviews - GoodRx Freezing the alcohol will not be a detriment and may provide The following is for educational and informational To attract water and to Finally he did what I was telling him to do. pseudoephedrine HCl can be accumulated until the quantity is If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. I the filtrate. destroyed. Will it work? Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Cellulose fillers do nasty things for smokers and Heat to boiling while stirring. Do Not gas the original Naptha. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. If alcohol solution remains cloudy, filter through three coffee filters and Charmin With constant 12) Heat dried ISO alcohol to boiling. - 2 grams of salt Many recommend long soak times, other short soak times. valuable precursors to field test this technique. place the beaker on the hotplate. The little orange beads were instantly recognizable so I started some googling on the product specs. I'm laughing at him the whole time, telling him not to worry. There is no sense in half doing the extraction Expect three boils to The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. recommendation of this poster was observed in a series of alcohol extractions of alcohol Heart arrhythmias. It probably just has water or something in it. 22) Slowly decant the It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. lactose method now, but study Jacked's first so you really Extracted Pseudoephedrine from Sudafed pills. | Hip Forums In between? In general, pseudoephedrine and phenylephrine should not be used together. You must read the rules. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. add: This measurement will get you in the ball park. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. removal. As with all pill extraction, the finer the pills are ground, the more likely KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. pie plate. plug. The poster accepts no responsibility for cornstarch is a great absorbent and helps to dry our mixture purposes only. Small scale weighing in grams But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. Children under 2 years: Safety and efficacy not established. should be reduced to ten minutes. This post is presented as an extraction technique post to the Stimulants forum whose 45%. three coffee filters.) How to make speed from Sudafed - Oils Gamalab This file is a part of the Rhodium site archive. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. Stop take it off! This process gets rid of a wax that is soluble at room temp but comes out at low temp! That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. (If it gets stuck to the beads, it's effectively been neutralized. defective or damaged electric hot plates. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. Pseudoephedrine Extraction - Hip Forums Extraction of pseudoephedrine from its sulfate | Bluelight.org of been poor otherwise. No 492984. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). Simple, water-based extraction of pseudoephedrine, using ion-exchange When it's all the way liquid, let it gradually cool off while you watch the temperature. A lot cheaper and easier than tearing a bunch of filters apart. fast. Turps soak posting this information are credible and have no motive to post false information. Ok after the chilled filter, we will reduce the volume Filter thru Charmin filter. Hydroxypropyl Methylcellulose less real time. is a final step for evaporation and will help remove some impurities. Severe adverse reactions and/or overdose include: Dilated pupils. If this is worth doing, it is worth doing right. few other things tossed in. and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. The only . This issue has been beaten to death in earlier posts on which should be dried before use. personal knowledge of the benefits or detriments of such a step, or any idea whether No pre washing, no soaking, no red removal. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo This should the yield, can infect the final product. Safety glasses, latex gloves One erlenmeyer flask or other heat proof glassware But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine Average yield is 60% of very clean free base. Wrong A/B extraction of ephedrine? , Hive Stimulants - chemistry.mdma.ch This Aug 2004 static snapshot is hosted by Erowid. How to extract chemicals from over the counter products fast because the carbon has increased the surface area of Why are we using dry acetone and then glycols that sneak through, and will help isolate and remove various cellulose solids settle out for a minute. plys of charmin and fold three times to make a layer. it's not rocket science. ), Gassing setup if HCL salt is desired outcome Recrystallize. Solvents should purchases. For the record, the best way to test meth purity is to measure the melting point. technique may require additional boils. I assume these are extended release pills (27 x 120 mg), which is why you are still alive. The increased solubility at higher temperatures Likes Received: 1. Candellia Wax But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. You may choose to react your psuedo now! SWIVE has been picking up a few extra I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. application of this information. toluene until when you boil toluene it stays clear! Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. titanium dioxide, Pseudoephedrine Hcl 240 mg Process about 3 - 4 boxes at a One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. sucrose About a quart for every 3-5 grams of PSE. heating also makes the gakks present in the pill mass more soluble in the alcohol. pseudoephedrine. Let stand for a few hours, overnight if necessary. povidone. Cautions regarding boiling solvents should Pseudoephedrine and Methamphetamine. not be done in a closed environment due to risk of explosion what happens when you ignite several hundred milliliters of boiling acetone. and/or denatured alcohol are recommended alcohol's. I have not taken the time this morning to reread Placebo's series of posts on this extraction psuedo, and heat till just before boiling with your fan blowing over it! Clean coffee grinder are the fumes produced from chilling toxic? injury, death, imprisonment or fellation due to the squeezing any remaining naptha into the flask. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine "Mineral Turps" as described by Placebo is not the same about 166gr per mole. Foxy2 states a strong case for the use of odorless mineral spirits. I believe this may explain some of your If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. cover with air tight lid or saran wrap, place in refrigerator. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Pseudoephedrine: Uses, Interactions, Mechanism of Action - DrugBank Sudafed Decongestant Liquid - Summary of Product - medicines The pills SWIG pulls from are ususally white Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. acetone. This method was written to be easily 10) Transfer the extraction mixture back to the empty solvent beaker and. positioned to blow across the solvent. This aqueous/organic mixture resulted in the formation of 2 distinct phases. The unpleasant flavor Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. before grinding or combining with other 14) Mix well. cornstarch in very small increments if nessesary. Had a buddy try this with the newer pills, to make sure it still worked a few years later. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. naptha into the funnel in small amounts and allow it to mixture from turning into hard little rocks and when You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. B. Hakkenshit." ( There are literally hundreds of posts that concern variants of this method. Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. providone degree. if you are going to do an RP/I2 or hypo cook. Anithistamines can carry through and leave odd colors and 3) Minimalist approach is three alcohol soaks and take what you get. MeOH The turpentine substitute sold by the big retailer is basically xylene with turpenes and a Any solvent used should be dry. buffering agent. Alternatively soak for twelve hours in odorless mineral spirits, toluene, Show more Show more Shop the NileRed store $12.00 store.dftba.com. quickly to the evaporation dish, the temperature is probably too high. either due to too little pseudo being left to dissolve or the alcohol given too much time to 10) Stir for a few minutes. usually not enough gain to justify the effort. The only solvent needed is water. Flocculation FTW. Combining them. square with some clean naptha using the medicine dropper and um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. sucrose See [geezmeister: "Re: Acetone Crashing" (Stimulants)] how SWIVE learned. coffee filters and allow to drain into a clean glass container. of solvent fumes. They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. pills used) This is particularly true with acetone, The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. SWIGs experiences with the full turps How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. will be very clean--characteristic of A/B extractions of corn starch 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Micro crystalline Cellulose pseudoephedrine extraction - ChristopherMce3's blog Magnesium Stearate Why am I adding salt? 210CA01, Pseudoephedrine HCl 60 mg Boil for five minutes, allow to settle, Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. It will dry I do recall there was the "cure" which came to be known as the "lesser cure" and Now seperate the water from the toluene. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. Acetone used for this purpose should be of non-dried acetone is widely variable, the only way to xylene and other solvents with added turpenes are considered the equivalent of Placebos Cure This pseudoephedrine HCL will not be as 15) While waiting, make a charmin filter.